Reagent generation assisted by ultrasonic irradiation
نویسندگان
چکیده
منابع مشابه
Ultrasonic Irradiation Assisted Enantioselective Synthesis of Alzheimer’s Disease Drug Rivastigmine Tartrate by Using Nanocatalyst
A highly efficient and convenient procedure for the enantioselective synthesis of (S)-Rivastigmine tartrate, a cholinergic agent for the treatment of mild to moderate dementia of the Alzheimer’s disease, is accomplished by the treatment of versatile, readily accessible N-Ethyl-N-methyl carbamoyl chloride with 3-hydroxyacetophenone under ultrasonic irradiation in presence of nano-K2CO3 were repo...
متن کاملUltrasonic irradiation assisted efficient regioselective synthesis of CF3-containing pyrazoles catalyzed by Cu(OTf)2/Et3N
BACKGROUND Most of the known approaches to the synthesis of CF3-containing organic compounds suffer from serious drawbacks. For example the starting materials required for these methods are rather difficult to obtain, or they are fairly toxic and inconvenient to work with and methods for direct fluorination and trifluoromethylation do not always allow the introduction of the CF3-group at the re...
متن کاملUltrasonic assisted-ECAP.
Equal channel angular pressing (ECAP) is one of the most prominent procedures for achieving ultra-fine grain (UFG) structures among the various severe plastic deformation (SPD) techniques. In this study, the effect of ultrasonic vibration on deformation behavior of commercial pure aluminum in the ECAP process is analyzed successfully using three dimensional (3D) by finite element methods (FEMs)...
متن کاملUltrasonic Assisted Preparation of Nano HMX
Size reduction of high energy materials such as 1, 3, 5, 7-tetranitro- 1, 3, 5, 7-tetraaza cyclooctane (HMX) has considerable influences on improving their explosive characteristics. In this study, nanosized HMX particles were produced using ultrasonically reprecipitation method by applying water as a safe and accessible antisolvent instead of unsafe conventional methods. SEM photographs revea...
متن کاملPreparation and Characterization of ZrO2/TiO2 Nanocomposite under Ultrasonic Irradiation by Sol-gel Route
TiO2/ZrO2 nanocomposite was obtained by the sonochemical technique. In this method, two separate gels containing zirconium and titanium were prepared and mixed together. The precursor sol of zirconium was prepared from an aqueous solution of ZrCl4. The precursor titanium tetra isopropoxide (TTIP) dissolved in isopropanol. Mixing of Titanium and Zirconium gels was resulted in a yellow TiO2/ZrO2 ...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Journal of the Brazilian Chemical Society
سال: 2003
ISSN: 0103-5053
DOI: 10.1590/s0103-50532003000200011